|Table of Contents|

Study on the Synthesis and Application of Flame Retardant Perchloropentacyclodecan(PDF)

南京师范大学学报（工程技术版）[ISSN:1006-6977/CN:61-1281/TN]

Issue:
2008年01期
Page:
55-58
Research Field:
Publishing date:

Info

Title:
Study on the Synthesis and Application of Flame Retardant Perchloropentacyclodecan
Author(s):
Li Li1; Yang Jinfei2; Zhu Yuan1
1.Department of Chemistry,Nanjing Xiaozhuang College,Nanjing 210041,China;2.School of Chemistry and Environmental Science,Nanjing Normal University,Nanjing 210097,China
Keywords:
flam e re tardant;  Perch lo ropentacyclodecan;  synthes is
PACS:
TQ314.248
DOI:
-
Abstract:
In th is paper, flam e re tardant Perch lo ropentacyclodecan is syn thesized by reaction o f hex ach lorocyclopentad iene through A lC l3 as the cata lyzer. In the course of synthes is, through the orthogonal design the var ious reaction cond-i tions are discussed. So the optim al reac tion cond itions a re confirm ed: the am ount of cata ly st is 1. 5 percent, reaction tim e is 2 hours, and the reaction tem pe rature is 90℃ . A t last, the perform ances in d ifferentm ater ia ls are tested. The resu lts show that Perch lo ropentacyclodecan is an effective flame re tardant for the po lym er ic ma teria ls.

References:

[ 1] 欧育湘. 阻燃剂— 制造、性能及应用[M ]. 北京: 化学工业出版社, 2007: 149- 150.
Ou Yux iang. Fire Re tardan t-M anufactu ring, Properties and App lications[M ]. Be ijing: Chem ica l Industry Press, 2007: 149- 150. ( in Ch inese)
[ 2] 王永强. 阻燃材料及应用技术[M ]. 北京: 化学工业出版社, 2003: 50- 65.
W ang Yongqiang. Flam e RetardantM a teria ls and Application Techno logy[M ] . Beijing: Chem ica l Industry Press, 2003: 50- 65. ( in Chinese)
[ 3] 杨栋梁. 含卤素的阻燃剂( Ⅱ ) [ J]. 印染, 1999, 25( 9): 41- 46.
Yang Dongliang. Key term s flam e re tardant ha logen m echan ism app ly ( Ⅱ ) [ J]. H a logen F lame Re tardan t, 1999, 25( 9 ): 41- 46. ( in Ch inese)
[ 4] 郑丽卿, 杨锦飞. 阻燃剂得克隆( DCRP)的合成[ J] . 南京师范大学学报: 工程技术版, 2003, 3( 4) : 15- 17.
Zheng L iq ing, Yang J infe.i S tudy on the synthesis of flam e re tardant DCRP [ J]. Journa l o f Nanjing Norm a l University: Eng-i neering and Techno logy Edition, 2003, 3( 4): 15- 17. ( in Ch inese)
[ 5] 张亨. 几种重要的有机氯系阻燃剂[ J]. 中国氯碱, 2002( 7): 25 -27.
ZhangH eng. Seve ra l importan t org an ic chloro-based fire retandants[ J]. China Ch lorA lka,i 2002( 7): 25- 27. ( in Chinese)
[ 6] 曾敏修. 双( 六氯环戊烯)环戊烷的合成及其应用[ J] . 阻燃材料与技术, 1989( 1): 12- 15.
Zeng M inx iu. Synthesis and app lication o f tw -i ( hexachloro cyc lopentene) cy clopen tane[ J]. F lam eReta rdantM ater ia l and Techno logy, 1989( 1): 12- 15. ( in Ch inese)
[ 7] 黄青松, 张军, 王立春, 等. 不同卤素阻燃剂协同阻燃LDPE的研究[ J] . 现代塑料加工应用, 2006, 18( 2): 39- 39.
H uang Q ingsong, Zhang Jun, W ang Lichun, et a.l Study on the flame retardancy o f LDPE w ith d ifferent ha logen flam e re tardants[ J]. M odern P lastics Pro cessing and Applications, 2006, 18( 2) : 39- 39. ( in Ch inese)
[ 8] H ayam ,i H iro sh ,i K iyoak,i e t a.l E lectrica lly insulated cable and a rrangement fo r connecting the cable: US, 6064002 [ P]. 2000-05-16.

Memo

Memo:
-
Last Update: 2013-04-24