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Study on Synthesis of Triphenyl Phosphate in Water(PDF)

南京师范大学学报(工程技术版)[ISSN:1006-6977/CN:61-1281/TN]

Issue:
2012年01期
Page:
85-87
Research Field:
Publishing date:

Info

Title:
Study on Synthesis of Triphenyl Phosphate in Water
Author(s):
Luo XuanShi HongliYang JinfeiZhi Huizhen
School of Chemistry and Materials Science,Nanjing Normal University,Nanjing 210097,China
Keywords:
watertriphenyl phosphatesynthesis
PACS:
TQ414
DOI:
-
Abstract:
The technological conditions of synthesis of triphenyl phosphate in water at room temperature were studied, and a better and easily industrialized process was found. When the reaction time is 2. 5 h and n( PhOH) ∶ n( NaOH) ∶ n ( POCl3 ) = 0. 90∶ 0. 99∶ 0. 33,91% yield can be obtained.

References:

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Last Update: 2013-03-11