[1]王东新.溶胶-凝胶气相色谱毛细管柱测定电热蚊香中的有效成分[J].南京师范大学学报(工程技术版),2002,02(03):070-73.
　Wang Dongxin.Determination of Prallethrin in Electrothermal Mosquito-repellent Incense by Adopting Sol-Gel Capillary Gas Chromatography[J].Journal of Nanjing Normal University(Engineering and Technology),2002,02(03):070-73.
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溶胶-凝胶气相色谱毛细管柱测定电热蚊香中的有效成分
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南京师范大学学报（工程技术版）[ISSN:1006-6977/CN:61-1281/TN]

卷:
02卷
期数:
2002年03期
页码:
070-73
栏目:
出版日期:
2002-09-30

文章信息/Info

Title:
Determination of Prallethrin in Electrothermal Mosquito-repellent Incense by Adopting Sol-Gel Capillary Gas Chromatography
作者:
王东新
南京师范大学化学与环境科学学院, 210097, 南京
Author(s):
Wang Dongxin
College of Chemistry and Environmental Science, Nanjing Normal University, 210097, Nanjing, RPC
关键词:
丙炔菊酯;  溶胶凝胶;  气相色谱
Keywords:
prallethrin;  sol-g el;  gas chromatog raphy
分类号:
O657.8
摘要:
采用新型高效耐高温溶胶 -凝胶气相色谱柱对电热蚊香片中的有效成分丙炔菊酯进行定量分析 ,以邻苯二甲酸二丁酯为内标 ,回收率为 10 0 .5 % ,相对标准偏差 (变异系数 )是 0 .92 % ,本方法简单而又准确可靠
Abstract:
A gas chromatogr aphic metho d with sol- gel capillary PDMS column for quantitative determination of prallethrin is r eported. Dibutyl phthalate is used as the inter nal standar d. The average recov er y is 100. 5% and the relativ e standar d deviation is 0. 92%. This method is simple and accurate.

参考文献/References:

[ 1] Wang Do ngx in. So-l Gel Chemistry-Mediated Novel Approach to Column Technology for High-Resolution Capillary Gas Chromatography [ Ph D Dissertation] [ D] . Tampa, Florida: Univ ersity of South Flor ida, 2000.
[ 2] Wang D, Chong S L, Malik A. So-l Gel Column Techno logy for Single- Step Deactivation, Coating, and Stationary- Phase Immobilization in High-Resolution Capillary Gas Chromatography[ J] . Anal Chem, 1997, 69: 4566~ 4576.
[ 3] 王东新, Malik A. 溶胶凝胶法制备用于分离极性有机化合物的毛细管气相色谱柱[ J] . 色谱, 2002, 20( 3) : 279~282.
[ 4] 明九雪, 钱传范. 电热蚊香液中右旋炔丙菊酯的气相色谱分析方法[ J] . 农药科学与管理, 1998, 67( 3) : 5.~ 72
[ 5] 郑曙昭, 李荣专, 黄宗平. 毛细管气相色谱法测定电热蚊香液中的丙炔菊酯[ J] . 分析测试技术与仪器, 2002, 8( 1) :45~ 47.

相似文献/References:

[1]吴秀红,王东新.耐高温三乙醇胺毛细管气相色谱柱的制作和测评[J].南京师范大学学报(工程技术版),2004,04(04):068.
　WU Xiuhong,WANG Dongxin.Making and Evaluating of Triethanol Amine Capillary Column for GC Used at High Temperatures[J].Journal of Nanjing Normal University(Engineering and Technology),2004,04(03):068.

备注/Memo

备注/Memo:
作者简介: 王东新, 1949- , 博士, 南京师范大学化学与环境科学学院副教授, 从事气相色谱柱的开发和应用研究.
基金项目: 南京师范大学留学回国人员启动基金( 项目编号: 2001HXXXGQB912)
更新日期/Last Update: 2013-04-29