[1]伏荣进,华毅超,司玮,等.LPG中化学添加剂的气相色谱分析[J].南京师范大学学报(工程技术版),2010,10(04):061-64.
 Fu Rongjin,Hua Yichao,Si Wei,et al.Analysis of Chemical Additives in LPG by GC[J].Journal of Nanjing Normal University(Engineering and Technology),2010,10(04):061-64.
点击复制

LPG中化学添加剂的气相色谱分析
分享到:

南京师范大学学报(工程技术版)[ISSN:1006-6977/CN:61-1281/TN]

卷:
10卷
期数:
2010年04期
页码:
061-64
栏目:
出版日期:
2010-12-31

文章信息/Info

Title:
Analysis of Chemical Additives in LPG by GC
作者:
伏荣进;华毅超;司玮;伊纪峰;
南京市产品质量监督检验院, 江苏南京210028
Author(s):
Fu RongjinHua YichaoSi WeiYi Jifeng
Nanjing Institute of Supervision and Testing on Product Quality,Nanjing 210028,China
关键词:
气相色谱 液化石油气 二甲醚
Keywords:
gas chrom atography liquefied pe tro leum gas d ime thy l ethe r
分类号:
TE626.7
摘要:
在原有液化石油气组成测定(色谱法)方法的基础上,采用气相色谱和双柱联用,通过对分析条件的优选,实现了LPG中化学添加剂的分离和定性、定量分析.结果表明:选用热导池检测器,控制气化温度、柱温等条件,LPG中DME等化学添加剂得到了较好的分离.此方法对原有仪器改动小,操作简便,分离效果好.
Abstract:
Gas chrom atography coup led w ith dua l??column was used to analyze the chem ica l add itives in the liquefied pe?? troleum gas based the or ig ina l chrom atography m ethod. The new m ethod pe rfo rm ed qualitative and quantitative ana lyses o f the chem ical add itives in LPG. The results show s that by se lecting therm a l conductiv ity detecto r, contro lling gas ifica?? tion and co lumn temperature, the chem ica l add itives, for ex amp le dim e thy l ether w ere iso la ted. The new m ethod w as h igh effec tive in separa tion, easy tom anipulate, and has alm ost no m od ification in the instruments.

参考文献/References:

[ 1] 项友谦, 王启. 二甲醚用作城镇燃气若干问题的探讨[ J]. 燃气技术, 2008, 404( 10) : 3-10. X iang Youq ian, W ang q.i DM E as a number o f issues o f urban gas[ J]. Gas Techno logy, 2008, 404( 10): 3-10. ( in Ch inese)
[ 2] 李浩春. 气相色谱法[M ]. 北京: 科技出版社, 1993. LiH aochun. Gas Chrom atography[M ]. Be ijing: Science and Techno logy Press, 1993. ( in Chinese)
[ 3] 李龙焕. 气相色谱法分析燃气组成[ J]. 科技资讯, 2009( 7): 110. Li Longhuan. G as ch rom a tog raphy ana ly sis of gas com position[ J]. Science and Techno logy Info rma tion, 2009( 7) : 110. ( in Chinese)
[ 4] 王红卫, 张晓冬, 丁黎, 等. 气相色谱法分析液化石油气组份的含量[ J]. 分析试验室, 2008, 27( S1): 276. W ang H ongw e,i Zhang X iaodong, Ding L,i e t a .l Gas chrom atography analysis of the con tent of liquefied petro leum gas compo?? nents[ J]. Chinese Journal o fAnalysis Labo ra to ry, 2008, 27( S1): 276. ( in Chinese)
[ 5] 金志刚. 燃气测试技术手册[M ]. 天津: 天津大学出版社, 1994. Jin Zh igang. Gas Test Techn ica lM anua l[M ]. Tianjin: T ianjin Univers ity Press, 1994. ( in Ch inese)
[ 6] 顾惠祥. 气相色谱实用手册[M ]. 2版. 北京: 化学工业出版社, 1990. Gu H u ix iang. Practica lM anua l GC[M ]. 2nd ed. Be ijing: Chem ica l Industry Press, 1990. ( in Ch inese)
[ 7] 许国旺. 现代实用气相色谱法[M ]. 北京: 化学工业出版社, 2004. Xu Guowang. M odern Prac tica lGas Chrom atog raphy[M ]. Be ijing: Chem ica l Industry Press, 2004. ( in Chinese)

相似文献/References:

[1]王东新.溶胶-凝胶聚二甲基硅氧烷毛细管气相色谱柱分析家用樟脑球的成份[J].南京师范大学学报(工程技术版),2005,05(04):065.
 WANG Dongxin.Determination of the Contents of Camphor Balls on a Sol-Gel PDMS Capillary Column for Gas Chromatography[J].Journal of Nanjing Normal University(Engineering and Technology),2005,05(04):065.

备注/Memo

备注/Memo:
基金项目: 南京市质量技术监督局科技项目. 通讯联系人: 伏荣进, 高级工程师, 研究方向: 各类气体产品的检验技术. Email:fu rongjin@ yeah. net
更新日期/Last Update: 2013-04-02