[1]刘国清,王玉萍,彭盘英,等.甲基磺酸钠酰氯化生产甲基磺酰氯的中控分析方法[J].南京师范大学学报(工程技术版),2011,11(03):055-58.
 Liu Guoqing,Wang Yuping,Peng Panying.A Method for Middle-controlled Analysis of Methanesulfonyl Chloride From Acid Chloride Reaction of Sodium Methanesulfonic Acid[J].Journal of Nanjing Normal University(Engineering and Technology),2011,11(03):055-58.
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甲基磺酸钠酰氯化生产甲基磺酰氯的中控分析方法
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南京师范大学学报(工程技术版)[ISSN:1006-6977/CN:61-1281/TN]

卷:
11卷
期数:
2011年03期
页码:
055-58
栏目:
出版日期:
2011-11-30

文章信息/Info

Title:
A Method for Middle-controlled Analysis of Methanesulfonyl Chloride From Acid Chloride Reaction of Sodium Methanesulfonic Acid
作者:
刘国清;王玉萍;彭盘英;
南京师范大学化学与材料科学学院,江苏南京210097
Author(s):
Liu GuoqingWang YupingPeng Panying
School of Chemistry and Material Science,Nanjing Normal University,Nanjing 210097,China
关键词:
甲基磺酰氯气相色谱法中控分析
Keywords:
methanesulfonyl chloridegas chromatographymiddle-controlled analysis
分类号:
TQ457.2
摘要:
采用气相色谱法测定甲基磺酸钠酰氯化反应产物中甲基磺酰氯的含量,计算甲基磺酰氯的收率,从而选择和控制酰氯化过程的工艺条件.该法具有分析速度快、操作简便、重现性好、准确度高等特点,可应用于对甲基磺酸钠酰氯化生产甲基磺酰氯的中控分析.
Abstract:
In the production of methanesulfonyl chloride from sodium methanesulfonic acid,the yield of methanesulfonyl chloride is determined through gas chromatography and calculated to help select and control the reaction conditions. This method is characterized by high speed analysis,simple operation,great reproducibility and high accuracy,and can be applied for the middle-controlled analysis of methanesulfonyl chloride in the acid chloride reaction.

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备注/Memo

备注/Memo:
基金项目: 江苏省自然科学基金( BK2009409) 、南京师范大学“211 工程”三期重点学科建设项目( 1843203623) 和江苏高校优势学科建设工程项目.通讯联系人: 彭盘英,教授,研究方向: 工业三废的治理与资源化. E-mail: pengpanying @ njnu. edu. Cn
更新日期/Last Update: 2013-03-21