[1]殷鹏飞,王声乐.大尺度Co9S8纳米线超声喷雾热解制备[J].南京师范大学学报(工程技术版),2006,06(04):050-52.
　YIN Pengfei,WANG Shengyue.Synthesis of the Wide Co9S8 Nanowires[J].Journal of Nanjing Normal University(Engineering and Technology),2006,06(04):050-52.
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大尺度Co9S8纳米线超声喷雾热解制备
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南京师范大学学报（工程技术版）[ISSN:1006-6977/CN:61-1281/TN]

卷:
06卷
期数:
2006年04期
页码:
050-52
栏目:
出版日期:
2006-12-30

文章信息/Info

Title:
Synthesis of the Wide Co9S8 Nanowires
作者:
殷鹏飞;王声乐;
东南大学物理系, 江苏南京210096
Author(s):
YIN Pengfei; WANG Shengyue
Department of Physics,Southeast University,Nanjing 210096,China
关键词:
Co9S8;  纳米线;  喷雾热解
Keywords:
Co9 S8;  nanow ires;  spray pyro lys is
分类号:
TB383.1
摘要:
以CoC l2.6H2O和CS(NH2)2为先驱物,运用超声喷雾热解法在300℃的玻璃衬底上成功地制备了Co9S8纳米线,所得Co9S8纳米线的直径约为500 nm.利用X射线衍射(XRD)、光学显微镜分别对产物的物相和形貌进行了表征,同时讨论了产生大尺度纳米线的软模板机理.
Abstract:
Co9S8 nanow ires w ere synthesized using coba lt ch lo ride ( CoC l2· 6H2O) and th iourea ( CS ( NH2 ) 2 ) as the sta rting m ater ia ls w ith the spray pyro lysis m ethod on g lass substrate at 300℃ w ith the diam eter o f about 500nm. The Co9 S8 sam ples w ere cha racte rized by X-ray d iffraction ( XRD) and optica l m icroscope respective ly, and a soft tem plate pr inciplew as d iscussed for the form ation o f thew ide Co9 S8 nanow ires.

参考文献/References:

[ 1] WOLD A, DW IGHT K. So lid State Chem istry [M ]. New York: Chapm an& H a ll Inc, 1993.
[ 2] CHAUKE H R, NGUYEN-MANH D, NGOEPE P E, et a.l E lectronic structure and stability of the pentlandites Co9 S8 and ( Fe, N i) 9 S8 [ J]. Phys Rev B, 2002, 66( 15): 155-105( 5).
[ 3] IGOR B, PAVEL A, M ICHEL D. Preparation of h ighly dispe rsed pentland ites (M, M’) 9 S8 (M, M’= Fe, Co, N i) and their ca talytic prope rties in hydrodesu lfur ization[ J]. J Phy s Chem B, 2004, 108( 23): 7 709-7 715.
[ 4] YAMADA H, TERAO K, AOKIM. E lectronic structure and m agnetic properties o fCoS2 [ J] . JM agnM agnM a ter, 1998, 177 181( Pa rt1): 607-608.
[ 5] SCHNEEMEYER L F, SIENKO M J. Crysta l data for m ix ed-an ion mo lybdenum d icha lcogen ides [ J]. Inorg Chem, 1980, 19( 3): 789-791.
[ 6] PASQUARIELLO D M, KERSHAW R, PASSARETT I J D, e t a.l Low-temperature synthesis and properties of Co9 S8, N i3 S2, and Fe7 S8 [ J]. Inorg Chem, 1984, 23( 7): 872-874.
[ 7] 张元广, 郭范, 万松明, 等. 水热法合成六角片状Co9 S8 晶体[ J] . 人工晶体学报, 2004, 33( 6): 927-929.
ZHANG Yuanguang, GUO Fan, WAN Songm ing, et a.l Hydrotherm a-l con tro lled synthesis o f hexagona l Co9 S8 sing le crystal flake[ J]. Journa l of Synthetic Crystals, 2004, 33( 6): 927-929. ( in Ch inese)
[ 8] LIU X H. H ydrothe rm al synthesis and character ization of nicke l and coba lt sulfides nanocrysta- llines[ J]. M at Sc i Eng B, 2005, 119( 1 3) : 19-24.
[ 9] WANG S Y, WANG W, LU ZH. Asynchronous-pu lse ultrason ic spray py ro ly sis deposition o f Cux S( x = /1, 2) th in film s[ J]. M a ter Sc i Eng B, 2003, 103( 2): 184-188.
[ 10] WANG W, WANG S Y, L IU M. Prepara tion o f γ- Gd2 S3 film s by u ltrasonic spray pyrolysis[ J]. M ate r Chem Phys, 2005, 94( 2 3) : 182-184.
[ 11] WANG W, WANG S Y, LIU M. G row th of rod- like crystal B iSI film s by u ltrasonic spray pyro lysis[ J]. M ate r Res Bul,l 2005, 40( 10): 1 781-1 786

相似文献/References:

[1]申秋芳,周晓锋,王声乐,等.大尺度NiS2纳米线的超声喷雾热解制备[J].南京师范大学学报(工程技术版),2008,08(02):059.
　Shen Qiufang,Zhou Xiaofeng,Wang Shengyue.Synthesis of Large-scale NiS2 Nanowires by Ultrasonic Spray Pyrolysis Method[J].Journal of Nanjing Normal University(Engineering and Technology),2008,08(04):059.

备注/Memo

备注/Memo:
基金项目: 江苏省自然科学基金资助项目( BK2004076) .
作者简介: 殷鹏飞( 1982-) , 硕士研究生, 主要从事纳米材料制备及物性方面的学习与研究. E-m ail:ch inese1002. s tuden ts@ sina. com
通讯联系人: 王声乐( 1964-) , 教授, 博士生导师, 主要从事纳米材料物理与化学方面的教学与研究. E-m ail:sywang@ seu. edu. cn
更新日期/Last Update: 2013-04-29